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By J R Partington

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Extra info for An Advanced Treatise on Physical Chemistry. Volume Two: The Properties of Liquids. First Edition.

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3 References p. 4 Sulfur(IV) Compounds Reactions of Sulflnyl Halides CF3S(O)F reacts with HF at 70°C (2 h) to give (C6 F5) 2S and C6F5S02F [29]. The reaction with (CF3hNO in presence of Hg and with LiN=C(CF3)2 gives (CF3)2NOS(O)CF3 [39] and CF3S(O)N=C(CF3b [28], respectively. The reaction with (CF3hC=NH in the presence of CsF yields CF3S(O)N=C(CF3h, (CF3hS=NCF(CF3)2 , CF3S(F)=NCF(CF3) 2 , CF3SN=C(CF3h, and (CF3hCFN=C(CF3)2 [56]. R1S(O)F (R1 = CF3, C2F5) reacts with HNF2 · KF and with HCl to yield RrSS0 2R1 and RrS(O)Cl [20], respectively.

Suppl. 3 References p. 45 44 Sulfur(IV) Compounds CF2ClSF3 reacts under mild conditions (20°C) with the walls of glas vessels to form CF2ClS(O)F. In presence of moisture the reaction proceeds due to the catalytic effect of produced HF to give CFCl3 and SF4 [51]. (CF3bSF2 reacts with anhydrous HCl according [61] (CF3bSF2 + 2 HCl---+ [(CF3bSCl2) + 2 HF 4 HF + Si02 ---+2 H2 0 +SiF4 [(CF3 bSC~] + H20---+ (CF3bSO + 2 HCl The reaction with NH3 in presence of C6H5 CH 2NH2 [43, 44], or with LiNH 2/NH 3 [48) gave (CF3bS=NH.

Denney, D. Z. Denney, Y. F. Hsu (J. Am. Chern. Soc. 95 [1973] 4064/5). J. Varwig, R. Mews (J. Chern. Res. (S) 1977 245, (M) 1977 2741/50). R. L. Kirchmeier, G. H. Sprenger, J. M. Shreeve (lnorg. Nucl. Chern. Letters 11 [1975] 699/703). [19] G. G. Furin, T. V. Terent'eva, A. I. Rezvukhin, G. G. Yakobson (lzv. Sibirsk. Otd. Akad. Nauk SSSR Ser. Khim. 6, pp. A. 82 [1975] No. 72600). [20] R. A. DeMarco, J. M. Shreeve (lnorg. Chern. 12 [1973]1896/9). [11] [12] [13] [14] [15] [16] [17] [18] (21] D. T.

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An Advanced Treatise on Physical Chemistry. Volume Two: The Properties of Liquids. First Edition. by J R Partington


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